油气太赫兹光谱仪时域谱的误差分析与标定STUDY ON ERROR ANALYSIS AND CALIBRATION OF TIME DOMAIN SPECTRUM OF OIL GAS TERAHERTZ SPECTROSCOPY
宝日玛,苗昕扬,陈星洁,王丹丹,詹洪磊,邢颖
摘要(Abstract):
在针对油气产品进行太赫兹光谱测试时,仪器自身误差会为测试结果来较大影响,对实验仪器进行误差标定对油气资源的太赫兹表征与精细评价具有重要意义。对油气太赫兹光谱仪进行了误差测试与分析,并对由延迟线的移动速度导致的测试误差进行了标定。结果表明,较小的移动速度有利于减少时域波形在延迟时间与幅值上产生的偏差及浮动,其中4组实验延迟时间的浮动范围分别为0.1Ps、0.1Ps、0.2Ps和0.4Ps;信号幅值的误差率分别为2.26%,1.76%,3.28%及5.82%。此外,在测试过程中,激光器输出功率的变化也是主要的误差来源,在测试时通过实时记录输出功率并根据线性关系进行归一化处理可降低这一误差。
关键词(KeyWords): 太赫兹光谱仪;延迟时间;幅值;误差分析
基金项目(Foundation): 教学改革项目:将科研思维及实践融入到大学物理教学过程的探索
作者(Author): 宝日玛,苗昕扬,陈星洁,王丹丹,詹洪磊,邢颖
参考文献(References):
- [1]杨玉平,张振伟.太赫兹成像技术[M].北京:中央民族大学出版社,2008:25-26,44-46,66-71.
- [2]BAO R M,Shixiang W,ZHAO K,et al.Applying terahertz time-domain spectroscopy to probe the evolution of kerogen in close pyrolysis systems[J].Science China Physics Mechanics&Astronomy,2013,56(8):1603-1605.
- [3]Bradley Ferguson,张希成.太赫兹科学与技术研究回顾[J].物理,2003(05):286-293.FERGUSON B,ZHANG X C.Materials for terahertz science and technology[J].Nature Materials,2003,1(1):26-33.(in Chinese)
- [4]GUO L,WANG X,HAN P,et al.Observation of dehydration dynamics in biological tissues with terahertz digital holography[Invited].[J].Applied Optics,2017,56(13):F173.
- [5]FENG X,WU S X,ZHAO K,et al.Pattern transitions of oil-water two-phase flow with low water content in rectangular horizontal pipes probed by terahertz spectrum[J].Optics express,2015,23(24):A1693-A1699.
- [6]ZHAN H,WU S,BAO R,et al.Qualitative identification of crude oils from different oil fields using terahertz time-domain spectroscopy[J].Fuel,2015,143:189-193.
- [7]ZHAN H,LI Q,ZHAO K,et al.Evaluating PM2.5at a construction site using terahertz radiation[J].IEEE Transactions on Terahertz Science&Technology,2015,5(6):1-7.
- [8]ZHAN H,ZHAO K,BAO R,et al.Monitoring PM2.5in the atmosphere by using terahertz time-domain spectroscopy[J].Journal of Infrared Millimeter&Terahertz Waves,2016,37(9):929-938.
- [9]MIAO X Y,ZHAN H L,ZHAO K.Application of THz technology in oil and gas optics[J].Science China Physics,Mechanics&Astronomy,2017,60(2):024231.
- [10]GUAN L M,ZHAN H L,MIAO X Y,et al.Terahertz-dependent evaluation of water content in high-water-cut crude oil using additive-manufactured samplers[J].Science China Physics,Mechanics&Astronomy,2017,60(4):044211.
- [11]孙青,邓玉强,于靖,等.基于气体特征吸收谱线的太赫兹时域光谱仪频率校准[J].应用光学,2012,03:554-557.SUN Q,DENG Y Q,YU J,et al.Frequency calibration of terahertz time-domain spectrometers using absorption lines of carbon monoxide[J].Journal of Applied Optics,2012,8195(4):81950N.(in Chinese)
- [12]刘传军,孙青,邓玉强,等.提高太赫兹时域光谱仪测量速度研究[J].光谱学与光谱分析,2015,12:3330-3333.LIU C J,SUN Q,DENG Y Q,et al.Research on improving the measurement speed of THz-TDS instruments[J].Spectroscopy&Spectral Analysis,2015,35(12):3330.(in Chinese)
- [13]ZHAN H L,SUN S N,ZHAO K,et al.Less than 6GHz resolution THz spectroscopy of water vapor[J].Science China Technological Sciences,2015,58(12):2104-2109.
- [14]Van Exter M,Grischkowsky D.Characterization of an optoelectronic terahertz beam system[J].Microwave Theory&Techniques IEEE Transactions on,1990,38(11):1684-1691.
- [15]徐新龙.从THz时间波形中提取材料参数的方法和分析[D].首都师范大学,2003.
- [16]ZHAN H L,ZHAO K,XIAO L Z.Non-contacting characterization of PM2.5in dusty environment with THz-TDS[J].Science China Physics Mechanics&Astronomy,2016,59(4):1-2.
- [17]汪景荣,张卓勇,张振伟,等.偏最小二乘法和THz-TDS在正品大黄鉴别中的应用[J].光谱学与光谱分析,2016,02:316-321.WANG J R,ZHANG Z Y,ZHANG Z W,et al.Identification of official rhubarb samples by using PLS and terahertz time-domain spectroscopy[J].Spectroscopy&Spectral Analysis,2016,36(2):316-321.(in Chinese)
- [18]赵昆,詹洪磊.太赫兹光谱分析技术[M].北京:科学出版社,2017.
- [19]ZHAN H,ZHAO K,ZHAO H,et al.The spectral analysis of fuel oils using terahertz radiation and chemometric methods[J].Journal of Physics D Applied Physics,2016,49(39).